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XRF Calibration Standard Guide
 

Xcalibur XRF Services calibration standards are provided by CalMetrics, Inc. a qualified and fully equipped standards calibration laboratory.

CalMetrics acquired exclusive licensed technology for standard development and manufacture from ThermoElectron, previously a division of Veeco Instruments and originally founded as UPA Technology. Now an independent company, the employees (qualified chemists) and owners have in excess of 20 years average experience in the EDXRF industry. With an extensive primary standard library, CalMetrics is capable of providing the best standards calibration service in the industry. Along with XRF standards they can also provide calibrations on thickness standards for beta back scatter, gauging sheets for magnetic lift off, eddy current standards and hall effect standards.

When ordering XRF standards please remember:

  1. Calibration standards come in two formats: Plated and Foil standards
    • Plated Standards: although more resilient are less versatile, as they are plated directly onto the base material. Some plated standards might also be susceptible to migration over time depending on the application.
    • Foil standards are more delicate and are more easily damaged through rough handling. Foil standards although more delicate are more versatile as the base material can be interchanged. Foil standards, depending on the type of mount, can be stacked. Stacked standards make it possible to calibrate multilayer applications.
  2. It is important to indicate the type of XRF system being used when ordering, as standards can be mounted to different platforms. Also, a flat mount would allow stacking of standards for a greater range of applications.
  3. Another reason to indicate the XRF system used is because the algorithms might vary from system to system (the Sn-Pb/Cu algorithm on a Veeco XRF is different than that of a Seiko SFT). This may mean the same calibration for two different systems might require a different range or quantity of standards.
  4. Foil Standard sets typically come with one base material. Alternate base material must be specified.
  5. Standards can also be made from customer-supplied samples, referred to as: T.S.P.S. (Thickness Standards Preparation Service), pricing for this available on a case-by-case basis.

RoHS and WEEE Standards:

Description

Format
Comments
WEE/ROHS PVC Contaminant 3 Pt. Set
32mm Round
contaminant values are listed for Br, Hg, Cr, Pb & Cd
WEE/ROHS PE Contaminant 3 Pt. Set
32mm Round
contaminant values are listed for Br, Hg, Cr, Pb & Cd
WEE/ROHS 8 96.5%Sn-3%Ag-0.5%Cu
Flat
-
WEE/ROHS 8 96.4%Sn-3%Ag-0.5%Cu+1000PPM Pb
Flat
-
WEE/ROHS 8 96.5%Sn-3%Ag-0.5%Cu
32mm Round
-
WEE/ROHS 8 96.4%Sn-3%Ag-0.5%Cu+1000PPM Pb
32mm Round
-
WEE/ROHS 8Sn + 1000PPM Pb
Flat
-
WEE/ROHS 8Sn + 1000PPM Pb
32mm Round
-

Thin Film Standards:

Description
Thickness
Comments
Au(Gold) Foils
starting at 30 Angstroms
-
Ag(Silver) Foils
starting at 500 Angstroms (2 uin)
-
Al(Aluminum) Foils
starting at 500 Angstroms (2uin)
-
Cr(Cromium) Foils
starting at 500 Angstroms (2uin)
-
Ni(Nickel) Foils
starting at 250 Angstroms (1uin)
-
Pd(Palladium) Foils
starting at 250 Angstroms (1uin)
-
Ti(Titanium) Foils
starting at 1000 Angstroms (4uin)
-
Co(Cobalt) Foils
starting at 1000 Angstroms (4uin)
-
Ti-W/Si Plated
starting at 1000 Angstroms (4uin)
Ti-W (10%-90%) Alloy
Cu/Si Plated
-
-
Ni-P/Si Plated
-
-

Special XRF Standards(other standards available upon request):

Application
Thickness Range
Comments
Pd-Ni Foil
-
Varied Pd composition
Au/Pd/Ni/Cu
-
-
Ni-P Foils
4% - 12%, 100uin - 500uin
-

Pd free Solder Standards:

Application
Thickness Range
Comments
Sn-Bi Foil
-
Can be purchased individually or in sets
Sn-Ag Foil
-
Can be purchased individually or in sets
Sn-Cu Foil
-
Can be purchased individually or in sets
Sn-Zn Foil
-
Can be purchased individually or in sets

Pure Element Standards for Elemental Analysis EDXRF systems:

Application
Comment
Infinite Element Kit (20 Elements Total)
For Elemental Analysis Systems (contact Xcalibur XRF for detail material)
Individual Element Standards
32mm round holder, Sample measurement surface area 0.7" x 0.7" sq (starting at element Na)

Precious Metal Alloy Standards(other standards can be special ordered and traceable to NIST):

Description
Details
Comments
10K Gold yellow
10 karat yellow 5 element
trace Indium
10K Gold white
10 karat white 5 element
0% Ag, trace Indium
14K Gold yellow
14 karat yellow 5 element
0% Ni, trace Iridium
14K Gold white
14 karat yellow 4 element
-
14K Gold white
14 karat yellow 4 element
-
14K Gold green
14 karat yellow 4 element
trace Zn
18K Gold yellow
18 karat yellow 4 element
trace Zn
18K Gold yellow
18 karat yellow 4 element
trace Zn
21K Gold yellow/pink
21 karat yellow 3 element
-
21K Gold white
21 karat white 2 element
Palladium
22K Gold yellow
22 karat yellow 4 element
trace Zn
Pt-Ir Platinum
90-10 to 98-2, Platinum-Iridium
Now Traceable to NIST
Pt-Ru Platinum
-
-

XRF standard range table (Proportional counter & SSD systems vary greatly in measureable range):

Application
XRF Range
Base Material
Comments
Au
<1 - 320 uin
Ni
special order thin Au, 0 - 5 uin
Ag
2 - 2000 uin
Cu
-
Al
2 - 4500 uin
Fe
Thin Al foils available
Cd
20 - 2000 uin
Fe
-
Cr
2 - 800 uin
Fe
special order thin Cr, 0 - 10 uin
Co
2 - 1200 uin
Fe
special order thin Co, 0 - 10 uin
Cu
2 - 1200 uin
Fe
Use Ni filter for Cu/Brass
Mo
20 - 2200 uin
Fe
special order thin Mo for Mo/Si
Ni-P
100 - 800 uin
Fe
specify P content when ordering
Ni
1 - 1000 uin
Cu
Use Co filter with Cu base material
Pd
1 - 250 uin
Ni
special order thin Pd, 0 - 10 uin
Rh
20 - 350 uin
Ni
special order thin Rh, 0 - 10 uin
Sn
2 - 2500 uin
Cu
special order thin Sn, 0 - 40 uin
Ti
4 - 1300 uin
Fe
-
Zn
20 - 1300 uin
Fe
-
Au/Ni/xx
Au: 20 - 100 uin
Ni: 10 - 300 uin
Cu
-
Au/Ni-P/xx
Au: 20 - 100 uin
Ni: 100 - 300 uin
Cu
specify P content when ordering
Au/Ni/xx (immersion)
Au: 1 - 15 uin
Ni: 10 - 400 uin
Cu
-
Au/Ni-P/xx (immersion)
Au: 1 - 15 uin
Ni: 10 - 400 uin
Cu
-
Au/Ag/xx
Au: 20 - 100 uin
Ag: 20 - 200 uin
Cu
-
Au/Pd/xx
Au: 10 - 100 uin
Pd: 2 - 300 uin
Ni
-
Ag/Ni/xx
Ag: 10 - 300 uin
Ni: 10 - 500 uin
Cu
-
Cr/Ni/xx
Cr: 30 - 200 uin
Ni: 20 - 500 uin
Fe
-
Cu-Zn/xx
0 - 100% Cu
10 - 500 uin
Fe
thickness and composition
Ni/Cu/xx
Ni: 20 - 650 uin
Cu: 20 - 700 uin
Fe
Ni or Co filters needed in measuring on Zn or Brass
Pd-Ni/xx
0 - 100% Pd
20 - 300 uin
Cu
thickness and composition
Pd/Ni/xx
Pd: 10 - 120 uin
Ni: 10 - 500 uin
Cu
-
Sn-Pb/xx
Sn Thickness 100%
40 - 3500 uin
Cu
numerical filtering required for PCB applications
"
Sn - Pb (60 - 40)
40 - 1500 uin
"
Sn-Pb/Ni/Ag/ Ceramic applications
"
Sn - Pb (90 - 10)
40 - 2000 uin
"
-
Sn/Ni/xx
Sn: 10 - 350 uin
Ni: 10 - 500 uin
Cu
-
Sn/Cu/xx
Sn: 10 - 350 uin
Cu: 10 - 500 uin
Fe
Ni filter needed when measuring on brass
Sn-Ni/xx
0 - 100% Sn
50 - 1000 uin
Cu
-
Zn-Ni/Fe
0 - 100% Zn
10 - 500 uin
Fe
-

Other Plated or Foil standards are available, if you can not find what you need on this list please contact us. Standards can also be made from customer supplied samples.

Other Base materials available: Cu, Al-1100, Al-2024, Al-3003, Alloy 42, Alloy 52, Brass, Cd, F@4-Epoxy, SS 304, Invar, Kovar, Ni, PBrnz, Pb, Sn Zn, Mo, Cu-clad Epoxy, Inconel 600, Monel

Base materials can also be made from customer supplied samples, contact us for more information

 

 

 
 
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